1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

Base Information

Chemical Name:1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one
CAS No.:1007346-42-0
Molecular Formula:C₁₇H₂₄BNO₃
Molecular Weight:301.193
Hs Code.:

Synonyms:1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

Suppliers and Price of 1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

There total 3 articles about 1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.1%

: 4509-90-4
5-bromovaleroyl chloride

: 214360-73-3
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

: 1007346-42-0
1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

Guidance literature:: 5-bromovaleroyl chloride; 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 18.5h;

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 21h;

Reference yield: 9.0%

: 1007346-42-0
1-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]piperidin-2-one

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In 1,4-dioxane; water; for 18h; Inert atmosphere; Reflux;