Technology Process of C45H53N5O9S
There total 16 articles about C45H53N5O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4-methyl-morpholine; benzotriazol-1-ol; HATU;
In
dichloromethane;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C
1.2: 4 h / 10 °C
1.3: pH 6 - 7
2.1: thionyl chloride / 1 h / Reflux
3.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
4.1: lithium hydroxide / tetrahydrofuran / 20 °C
4.2: pH < 7
5.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
With
4-methyl-morpholine; thionyl chloride; benzotriazol-1-ol; HATU; lithium hydroxide; sodium t-butanolate;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium acetate / acetone
2.1: acetic acid; phosphoric acid / 5 h / Reflux
3.1: trichlorophosphate / 2 h / Reflux
4.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C
4.2: 4 h / 10 °C
4.3: pH 6 - 7
5.1: thionyl chloride / 1 h / Reflux
6.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
7.1: lithium hydroxide / tetrahydrofuran / 20 °C
7.2: pH < 7
8.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
With
4-methyl-morpholine; thionyl chloride; phosphoric acid; potassium acetate; benzotriazol-1-ol; acetic acid; HATU; lithium hydroxide; sodium t-butanolate; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetone;