6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

Base Information

Chemical Name:6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A
CAS No.:134160-32-0
Molecular Formula:C₇₄H₈₇FN₄O₂₂S₄
Molecular Weight:1531.78
Hs Code.:

Synonyms:6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

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Chemical Property of 6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

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Technology Process of 6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

There total 1 articles about 6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-24-7
acetic anhydride

: 134160-31-9
2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

: 134160-32-0
6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

Guidance literature:: With pyridine; dmap; for 5h; Ambient temperature;
DOI:10.1016/0008-6215(91)80124-6

Reference yield:

: 134160-32-0
6',3''-di-N-acetyl-5,2''-di-O-acetyl-2',4'-di-O-benzyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

: 134160-34-2
3''-N-acetyl-5,4',2''-tri-O-acetyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

: 134160-33-1
6',3''-di-N-acetyl-5,2''-di-O-acetyl-4'',6''-O-cyclohexylidene-3'-deoxy-3'-fluoro-1,3,6',3''-tetra-N-tosylkanamycin A

Guidance literature:: With hydrogen; palladium; In 1,4-dioxane; for 2h; under 760 Torr; Yields of byproduct given; Ambient temperature;
DOI:10.1016/0008-6215(91)80124-6