dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

Base Information

Chemical Name:dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)
CAS No.:1029056-55-0
Molecular Formula:C₁₉H₂₂Cl₂FeN₂
Molecular Weight:405.15
Hs Code.:

Synonyms:dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

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Chemical Property of dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

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Technology Process of dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

There total 1 articles about dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 78788-25-7
2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene

: iron(II) chloride

: 1029056-55-0
dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

Guidance literature:: In tetrahydrofuran; under Ar; FeCl2 added to soln. of ligand in THF; stirred at room temp. for 20 h; solvent removed by evapn. under reduced pressure; washed with toluene; elem. anal.;
DOI:10.1021/ic7022693

Reference yield: 80.0%

: 1029056-55-0
dichloro(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene)iron(II)

: 78788-25-7
2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene

: bis(2-methyl-1,4-bis(2,6-dimethylphenyl)-1,4-diaza-1,3-butadiene^(1-))iron(II)

Guidance literature:: With sodium; In hexane; under Ar; Na added to soln. of Fe complex in n-hexane with stirring at 20°C; stirred for 10 min; soln. of ligand in n-hexane added; stirred for 24 h; solvent removed by evapn. under reduced pressure; washed with MeCN; dried in vac.; elem. anal.;
DOI:10.1021/ic7022693