2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)
CAS No.:150196-32-0
Molecular Formula:C₂₂H₂₈O₈S₂
Molecular Weight:484.592
Hs Code.:2932990090

Synonyms:2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Suppliers and Price of 2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

There total 4 articles about 2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 900782-31-2
2-(tetrahydro-2H-pyran-2-yloxy)propane-1,3-diyl diacetate

: 150196-32-0
2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia / methanol / 20 °C

2: 6.1 g / pyridine

With pyridine; ammonia; In methanol;
DOI:10.1002/jlcr.1001

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 150196-32-0
2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / pyridinium p-toluenesulfonate / tetrahydrofuran / 3 h / 20 °C

2: 77 percent / tetra-n-butylammonium iodide; potassium carbonate / acetonitrile / 20 °C

3: ammonia / methanol / 20 °C

4: 6.1 g / pyridine

With pyridine; ammonia; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1002/jlcr.1001

Reference yield:

: 26562-22-1
2-<2-Bromo-1-(bromomethyl)ethoxy>tetrahydropyran

: 150196-32-0
2-((tetrahydro-2H-pyran-2-yl)oxy)propane-1,3-diyl bis(4-methylbenzenesulfonate)

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / tetra-n-butylammonium iodide; potassium carbonate / acetonitrile / 20 °C

2: ammonia / methanol / 20 °C

3: 6.1 g / pyridine

With pyridine; ammonia; tetra-(n-butyl)ammonium iodide; potassium carbonate; In methanol; acetonitrile;
DOI:10.1002/jlcr.1001