di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

Base Information

Chemical Name:di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate
CAS No.:1278587-05-5
Molecular Formula:C₂₃H₃₅NO₈
Molecular Weight:453.533
Hs Code.:

Synonyms:di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

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Chemical Property of di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

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Technology Process of di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

There total 5 articles about di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1278587-04-4
methyl 2-(2-(2-aminoethoxy)phenoxy)acetate

: 1278587-05-5
di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

Guidance literature:: methyl 2-(2-(2-aminoethoxy)phenoxy)acetate; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

bromoacetic acid tert-butyl ester; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1002/chem.201001548

Reference yield:

: 1278587-02-2
tert-butyl 2-(2-(benzyloxy)phenoxy)ethylcarbamate

: 1278587-05-5
di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol / 8 h / 20 °C / 2068.65 Torr / Inert atmosphere

2.1: potassium carbonate / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

2.2: 20 - 80 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

4.2: 60 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; trifluoroacetic acid; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201001548

Reference yield:

: 115499-56-4
tert-butyl 2-(2-hydroxyphenoxy)ethylcarbamate

: 1278587-05-5
di-tert-butyl 2,2'-(2-(2-(2-methoxy-2-oxoethoxy)phenoxy)ethylazanediyl)diacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetonitrile / 0.5 h / 20 °C / Inert atmosphere

1.2: 20 - 80 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

3.2: 60 °C

With potassium carbonate; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201001548