O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

Base Information

Chemical Name:O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol
CAS No.:123487-63-8
Molecular Formula:C₉₈H₁₀₇NO₂₇
Molecular Weight:1730.92
Hs Code.:

O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

Synonyms:O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

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Chemical Property of O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

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Technology Process of O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

There total 2 articles about O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀₀H₁₀₈ClNO₂₈

: 123487-63-8
O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

Guidance literature:: With thiourea; In ethanol; for 1h; Yield given; Heating;
DOI:10.1021/ja00110a011

Reference yield:

: 123487-57-0
Chloro-acetic acid (2S,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-pent-4-enyloxy-tetrahydro-pyran-3-yl ester

: 123487-59-2
O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

: 123487-63-8
O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; thiourea; Yield given. Multistep reaction; 1.) CH₂Cl₂, 2.) EtOH, reflux;
DOI:10.1021/ja00204a049

Reference yield: 68.0%

: 123487-63-8
O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-penta-O-acetyl-D-myo-inositol

: 123487-55-8
3,4,6-tri-O-benzoyl-β-D-mannopyranose 1,2-(pent-4-enyl orthobenzoate)

: 123487-62-7,123538-45-4
O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1-2)-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1-6)-O-(2,3,4-tri-O-benzyl-α-D-mannopyranosyl)-(1-4)-O-(3,6-di-O-benzyl-2-<(benzyloxycarbonyl)amino>-2-deoxy-α-D-glucopyranosyl)-(1-6)-1,2,3,4,5-pent

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/ja00204a049