Technology Process of C25H28O7
There total 8 articles about C25H28O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
at 0 ℃;
for 1h;
stereoselective reaction;
Inert atmosphere;
DOI:10.1021/ol402021e
- Guidance literature:
-
Multi-step reaction with 5 steps
1: iodine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2: 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 0 °C / Inert atmosphere; Reflux
3: dirhodium tetraacetate / dichloromethane / Inert atmosphere
4: N-iodo-succinimide; water / 1,4-dioxane / 0 - 20 °C / Inert atmosphere
5: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 0 °C / Inert atmosphere
With
dirhodium tetraacetate; N-iodo-succinimide; water; iodine; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
1,4-dioxane; dichloromethane; toluene;
DOI:10.1021/ol402021e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dirhodium tetraacetate / dichloromethane / Inert atmosphere
2: N-iodo-succinimide; water / 1,4-dioxane / 0 - 20 °C / Inert atmosphere
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1 h / 0 °C / Inert atmosphere
With
dirhodium tetraacetate; N-iodo-succinimide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
1,4-dioxane; dichloromethane;
DOI:10.1021/ol402021e
