(2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

Base Information

Chemical Name:(2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester
CAS No.:316172-62-0
Molecular Formula:C₁₇H₂₅NO₆
Molecular Weight:339.389
Hs Code.:

Synonyms:(2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

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Chemical Property of (2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

Chemical Property:

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Technology Process of (2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

There total 5 articles about (2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-4-((S)-Benzyloxy-methoxycarbonyl-methyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 316172-62-0
(2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

Guidance literature:: With methanol; hydrogen cation;
DOI:10.1016/S0960-894X(00)00487-X

Reference yield:

: 768387-35-5
(4R)-4-(1-hydroxy-allyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 316172-62-0
(2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / NaH; nBu₄NI

2: OsO₄; NaIO₄

3: Jones reagent

5: H⁺; MeOH

With methanol; sodium periodate; osmium(VIII) oxide; jones reagent; hydrogen cation; tetra-(n-butyl)ammonium iodide; sodium hydride; 1: Alkylation / 2: oxidative cleavage / 3: Oxidation / 4: Methylation / 5: acidolysis;
DOI:10.1016/S0960-894X(00)00487-X

Reference yield:

: 4-(1-benzyloxy-2-oxo-ethyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 316172-62-0
(2S,3R)-2-Benzyloxy-3-tert-butoxycarbonylamino-4-hydroxy-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Jones reagent

3: H⁺; MeOH

With methanol; jones reagent; hydrogen cation; 1: Oxidation / 2: Methylation / 3: acidolysis;
DOI:10.1016/S0960-894X(00)00487-X