C₃₃H₃₅BrN₂O₅

Base Information

Chemical Name:C₃₃H₃₅BrN₂O₅
CAS No.:1266096-67-6
Molecular Formula:C₃₃H₃₅BrN₂O₅
Molecular Weight:619.555
Hs Code.:

C<sub>33</sub>H<sub>35</sub>BrN<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₃H₃₅BrN₂O₅

Suppliers and Price of C₃₃H₃₅BrN₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₃₃H₃₅BrN₂O₅

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₃₃H₃₅BrN₂O₅

There total 11 articles about C₃₃H₃₅BrN₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1266100-24-6
C₃₅H₃₉BrN₂O₅

: 1266096-67-6
C₃₃H₃₅BrN₂O₅

Guidance literature:: With Umicore M₃₁; In dichloromethane; at 40 ℃; for 24h; Inert atmosphere;

Reference yield:

: 1199-90-2
1-(but-3-en-1-yl)-3-methoxybenzene

: 1266096-67-6
C₃₃H₃₅BrN₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron tribromide / dichloromethane / 3 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / chloroform / 20 h / 20 °C / Inert atmosphere

3.1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane; ethyl acetate / 0.75 h / 20 °C

4.1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 0 °C

5.1: Umicore M₃₁ / dichloromethane / 24 h / 40 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; 1,3-dimethylbarbituric acid; Umicore M₃₁; boron tribromide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; 1,1'-azodicarbonyl-dipiperidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; 2.1: Mitsunobu reaction;

Reference yield:

: 1266099-80-2
C₂₆H₃₀BrNO₄

: 1266096-67-6
C₃₃H₃₅BrN₂O₅

Guidance literature:: Multi-step reaction with 3 steps

1: 1,3-dimethylbarbituric acid / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane; ethyl acetate / 0.75 h / 20 °C

2: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 0 °C

3: Umicore M₃₁ / dichloromethane / 24 h / 40 °C / Inert atmosphere

With 1-hydroxy-7-aza-benzotriazole; 1,3-dimethylbarbituric acid; Umicore M₃₁; N-ethyl-N,N-diisopropylamine; HATU; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;