(2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal

Base Information

Chemical Name:(2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal
CAS No.:1197360-29-4
Molecular Formula:C₂₁H₃₀O₄
Molecular Weight:346.467
Hs Code.:

Synonyms:(2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal

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Chemical Property of (2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal

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Technology Process of (2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal

There total 1 articles about (2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1197360-47-6
C₂₁H₃₂O₄

: 1197360-29-4
(2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 3h;
DOI:10.1021/jo901913h

Reference yield: 81.0%

: 1197360-29-4
(2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal

: 51233-80-8
2,6-dimethylphenyl propionate

: 1197360-41-0
2,6-dimethylphenyl (2R,3R,4R,5R,6R)-5-(benzyloxy)-6-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxabicyclo[3.2.1]octan-3-yl)-3-hydroxy-2,4-dimethylheptanoate

Guidance literature:: 2,6-dimethylphenyl propionate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h;

(2S,3S,4R)-3-(benzyloxy)-4-((1S,3R,4R,5S)-1,4-dimethyl-2,8-dioxa-bicyclo[3.2.1]octan-3-yl)-2-methylpentanal; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

With water; ammonium chloride; In tetrahydrofuran; hexane; optical yield given as %de;
DOI:10.1021/jo901913h