Technology Process of 1-tosyloxy-3,7-dimethyl-6-octene-2-one
There total 7 articles about 1-tosyloxy-3,7-dimethyl-6-octene-2-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
diethyl ether;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 67 percent / KOH / ethane-1,2-diol; H2O; ethanol / 18 h / Heating
2: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature
3: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature
4: 82 percent / diethyl ether / Ambient temperature
With
pyridine; potassium hydroxide; oxalyl dichloride; triethylamine;
In
diethyl ether; ethanol; water; ethylene glycol; benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 42 percent / PBr3, pyridine / diethyl ether
2: 60 percent / dimethylsulfoxide
3: 67 percent / KOH / ethane-1,2-diol; H2O; ethanol / 18 h / Heating
4: 86 percent / oxalyl chloride, pyridine / benzene / 2 h / Ambient temperature
5: 76 percent / triethyl amine / diethyl ether / 1 h / Ambient temperature
6: 82 percent / diethyl ether / Ambient temperature
With
pyridine; potassium hydroxide; oxalyl dichloride; phosphorus tribromide; triethylamine;
In
diethyl ether; ethanol; water; ethylene glycol; dimethyl sulfoxide; benzene;
