N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

Base Information

Chemical Name:N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide
CAS No.:619297-34-6
Molecular Formula:C₂₄H₁₉BrN₂O₅S
Molecular Weight:527.395
Hs Code.:

<i>N</i>-[2-(1-benzenesulfonyl-1<i>H</i>-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

Synonyms:N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

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Technology Process of N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

There total 4 articles about N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 565184-70-5
N-[2-(1-benzenesulfonyl-3-phenylsulfanyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

: 619297-34-6
N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

Guidance literature:: nickel; In ethanol; for 1h; Heating;
DOI:10.1081/SCC-120021513

Reference yield:

: 85678-42-8
2-(bromomethyl)-3-(phenylthio)-1-(phenylsulfonyl)-1H-indole

: 619297-34-6
N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: aq. potassium carbonate / acetonitrile / 3 h / Heating

2: 85 percent / BF₃*Et₂O; MgSO₄ / CHCl₃ / 3 h / Heating

3: 50 percent / CrO₃*2Py / pyridine / 48 h / 50 - 60 °C

4: 85 percent / Raney nickel / ethanol / 1 h / Heating

With boron trifluoride diethyl etherate; dipyridine chromium trioxide; magnesium sulfate; potassium carbonate; nickel; In pyridine; ethanol; chloroform; acetonitrile;
DOI:10.1081/SCC-120021513

Reference yield:

: 147251-92-1
1-phenylsulfonyl-3-phenylthioindol-2-ylmethanol

: 619297-34-6
N-[2-(1-benzenesulfonyl-1H-indole-2-carbonyl)-4-bromo-5-methoxy-phenyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / BF₃*Et₂O; MgSO₄ / CHCl₃ / 3 h / Heating

2: 50 percent / CrO₃*2Py / pyridine / 48 h / 50 - 60 °C

3: 85 percent / Raney nickel / ethanol / 1 h / Heating

With boron trifluoride diethyl etherate; dipyridine chromium trioxide; magnesium sulfate; nickel; In pyridine; ethanol; chloroform;
DOI:10.1081/SCC-120021513