Salicylaldehyde isonicotinoyl hydrazone

Base Information

• Chemical Name: Salicylaldehyde isonicotinoyl hydrazone
• CAS No.: 495-84-1
• Molecular Formula: C13H11 N3 O2
• Molecular Weight: 241.249
• Hs Code.: 2934999090
• DSSTox Substance ID: DTXSID0046272
• Mol file: 495-84-1.mol

Synonyms:salicylaldehyde isonicotinoyl hydrazone;SIH cpd

Chemical Property of Salicylaldehyde isonicotinoyl hydrazone

Chemical Property:

• Melting Point: 232-233ºC
• Refractive Index: 1.623
• Boiling Point: 401.8°Cat760mmHg
• Flash Point: 196.8°C
• PSA: 74.58000
• Density: 1.24 g/cm³
• LogP: 1.94200
• Storage Temp.: -196°C
• XLogP3: 1.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 241.085126602
• Heavy Atom Count: 18
• Complexity: 301

Purity/Quality:

97% ^*data from raw suppliers

AT1 ≥98%(HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NNC(=O)C2=CC=NC=C2)O

Technology Process of Salicylaldehyde isonicotinoyl hydrazone

There total 19 articles about Salicylaldehyde isonicotinoyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

isoniazid (54-85-3,7640-37-1) + salicylaldehyde (90-02-8) → salicylaldehyde isonicotinoylhydrazone (495-84-1)

Guidance literature:

at 56 ℃; for 0.333333h;

DOI:10.1021/cg400529s

Reference yield: 98.7%

isoniazid (54-85-3,7640-37-1) + salicylaldehyde (90-02-8) → salinazid (495-84-1)

Guidance literature:

In ethanol; water; at 20 ℃; for 0.0833333h; UV-irradiation;

DOI:10.2174/1570178613666160824123827

Reference yield: 98.0%

isoniazid (54-85-3,7640-37-1) + 2-methyl-benzyl alcohol (89-95-2) → salinazid (495-84-1)

Guidance literature:

In acetate buffer; at 100 ℃; for 0.0666667h; pH=4.5;

DOI:10.1021/ja064806w

upstream raw materials:

isoniazid

salicylaldehyde

2-methyl-benzyl alcohol

pyridine-4-carboxylic acid

Downstream raw materials:

{Ag(C₇H₆ONNH(CO)C₅H₄N)2NO₃}

{Ag(C₇H₆ONNH(CO)C₅H₄N)2ClO₄}

bis(isonicotinamidosalicylaldimine)diacetatodioxouranium(VI)

bis(isonicotinamidosalicylaldimine)diiododioxouranium(VI)

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