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C38H45NO7

Base Information
  • Chemical Name:C38H45NO7
  • CAS No.:134733-92-9
  • Molecular Formula:C38H45NO7
  • Molecular Weight:627.778
  • Hs Code.:
C<sub>38</sub>H<sub>45</sub>NO<sub>7</sub>

Synonyms:C38H45NO7

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Chemical Property of C38H45NO7
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Technology Process of C38H45NO7

There total 11 articles about C38H45NO7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With bis(triphenylphosphine)nickel(II) chloride; triphenylphosphine; zinc; In N,N-dimethyl-formamide; at 50 ℃; for 21h;
Guidance literature:
Multi-step reaction with 10 steps
1: 1. HgO (yellow) / 1. CH2Cl2, 30min, 2. CHCl3, reflux, 24h
2: 1. m-chloroperoxybenzoic acid (MCPBA) / 1. CHCl2, r.t., 1h; 2. CHCl3, reflux, 40h
3: 74 percent / Zn, ethylenediaminetetraacetic acid / acetic acid; ethanol / 0.5 h / Heating
4: 31 percent / triethylamine / benzene / 8 h
5: methanolic KOH
6: 96 percent / pyridine / 4-Dimethylaminopyridine (DMAP) / 24 h
7: H2 / 5percent Pd/C / methanol; diethyl ether / 1.5 h / 760 Torr
8: K2CO3 / acetone / 4 h / Heating
9: 83 percent / I2, silver trifluoroacetate / CH2Cl2; CHCl3 / 3 h / Ambient temperature
10: 55 percent / bis(triphenylphosphine)nickel dichloride, Zn, triphenylphosphine / dimethylformamide / 21 h / 50 °C
With pyridine; potassium hydroxide; bis(triphenylphosphine)nickel(II) chloride; ethylenediaminetetraacetic acid; hydrogen; iodine; silver trifluoroacetate; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; mercury(II) oxide; zinc; dmap; palladium on activated charcoal; In methanol; diethyl ether; ethanol; dichloromethane; chloroform; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
Guidance literature:
Multi-step reaction with 10 steps
1: 1. HgO (yellow) / 1. CH2Cl2, 30min, 2. CHCl3, reflux, 24h
2: 1. m-chloroperoxybenzoic acid (MCPBA) / 1. CHCl2, r.t., 1h; 2. CHCl3, reflux, 40h
3: 74 percent / Zn, ethylenediaminetetraacetic acid / acetic acid; ethanol / 0.5 h / Heating
4: 31 percent / triethylamine / benzene / 8 h
5: methanolic KOH
6: 96 percent / pyridine / 4-Dimethylaminopyridine (DMAP) / 24 h
7: H2 / 5percent Pd/C / methanol; diethyl ether / 1.5 h / 760 Torr
8: K2CO3 / acetone / 4 h / Heating
9: 83 percent / I2, silver trifluoroacetate / CH2Cl2; CHCl3 / 3 h / Ambient temperature
10: 55 percent / bis(triphenylphosphine)nickel dichloride, Zn, triphenylphosphine / dimethylformamide / 21 h / 50 °C
With pyridine; potassium hydroxide; bis(triphenylphosphine)nickel(II) chloride; ethylenediaminetetraacetic acid; hydrogen; iodine; silver trifluoroacetate; potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; mercury(II) oxide; zinc; dmap; palladium on activated charcoal; In methanol; diethyl ether; ethanol; dichloromethane; chloroform; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
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