(2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

Base Information

Chemical Name:(2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide
CAS No.:647015-17-6
Molecular Formula:C₂₁H₃₅NO₇
Molecular Weight:413.511
Hs Code.:

Synonyms:(2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

Suppliers and Price of (2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Useful:

Technology Process of (2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

There total 1 articles about (2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 400737-43-1
(2R,3S,4R,5R,7R)-5-(tert-Butyl-dimethyl-silanyloxy)-3-hydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

: 647015-17-6
(2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 25 ℃; for 12h;
DOI:10.1021/ja030496v

Reference yield:

: 647015-17-6
(2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

: 647015-18-7
(3R,4S,5R,6R)-4-Hydroxy-6-[(R)-3-methoxy-2-(4-methoxy-benzyloxy)-propyl]-3,5-dimethyl-tetrahydro-pyran-2-one

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ja030496v

Reference yield:

: 647015-17-6
(2R,3S,4S,5R,7R)-3,5-Dihydroxy-8-methoxy-7-(4-methoxy-benzyloxy)-2,4-dimethyl-octanoic acid methoxy-methyl-amide

: 647015-21-2
(3R,4S,5S,6R)-6-[(R)-3-Methoxy-2-(4-methoxy-benzyloxy)-propyl]-3,5-dimethyl-4-triethylsilanyloxy-tetrahydro-pyran-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 600 mg / TFA / tetrahydrofuran / 1 h / 0 °C

2: 87 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / 25 °C

With 2,6-dimethylpyridine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja030496v