C₂₄H₄₁NO₃Si

Base Information

Chemical Name:C₂₄H₄₁NO₃Si
CAS No.:1358526-92-7
Molecular Formula:C₂₄H₄₁NO₃Si
Molecular Weight:419.68
Hs Code.:

C<sub>24</sub>H<sub>41</sub>NO<sub>3</sub>Si

Synonyms:C₂₄H₄₁NO₃Si

Suppliers and Price of C₂₄H₄₁NO₃Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of C₂₄H₄₁NO₃Si

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of C₂₄H₄₁NO₃Si

There total 8 articles about C₂₄H₄₁NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₃₅NOSi

: 501-53-1,94274-21-2
benzyl chloroformate

: 1358526-92-7
C₂₄H₄₁NO₃Si

Guidance literature:: With potassium carbonate; In tetrahydrofuran; water; at 0 ℃; for 1h;
DOI:10.1021/jo202350z

Reference yield:

: C₂₉H₄₃NO₄Si

: 1358526-92-7
C₂₄H₄₁NO₃Si

Guidance literature:: Multi-step reaction with 8 steps

1: deuterated DMF / 1.5 h / 70 °C

2: hydrogen / ethanol / 2 h / 20 °C

3: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 2 h / 0 °C

4: dmap; triethylamine / dichloromethane / 2 h / 20 °C

5: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide / 1,2-dimethoxyethane / 3 h / 80 °C

6: hexane; toluene / 2 h / 0 - 20 °C

7: 20 % Pd(OH)2/C; hydrogen / methanol / 12 h / 20 °C / 7600.51 Torr / Autoclave

8: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C

With dmap; 2,2'-azobis(isobutyronitrile); 20 % Pd(OH)2/C; hydrogen; tri-n-butyl-tin hydride; potassium carbonate; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; deuterated DMF; water; toluene;
DOI:10.1021/jo202350z

Reference yield:

: C₂₉H₄₃NO₄Si

: 1358526-92-7
C₂₄H₄₁NO₃Si

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogen / ethanol / 2 h / 20 °C

2: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 2 h / 0 °C

3: dmap; triethylamine / dichloromethane / 2 h / 20 °C

4: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide / 1,2-dimethoxyethane / 3 h / 80 °C

5: hexane; toluene / 2 h / 0 - 20 °C

6: 20 % Pd(OH)2/C; hydrogen / methanol / 12 h / 20 °C / 7600.51 Torr / Autoclave

7: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C

With dmap; 2,2'-azobis(isobutyronitrile); 20 % Pd(OH)2/C; hydrogen; tri-n-butyl-tin hydride; potassium carbonate; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; toluene;
DOI:10.1021/jo202350z