octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside
CAS No.:849208-06-6
Molecular Formula:C₄₈H₆₁N₃O₁₂S
Molecular Weight:904.091
Hs Code.:

Synonyms:octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

There total 1 articles about octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 849208-01-1
octyl 2-azido-2-deoxy-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 98-59-9
p-toluenesulfonyl chloride

: 849208-06-6
octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tetasy.2004.11.063

Reference yield: 85.0%

: 849208-06-6
octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 849208-07-7
octyl 2,6-diazido-2,6-dideoxy-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: With sodium azide; 15-crown-5; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1016/j.tetasy.2004.11.063

Reference yield:

: 849208-06-6
octyl 2-azido-2-deoxy-6-O-p-toluenesulfonyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-benzyl-α-D-mannopyranoside

: 849208-08-8
N-[(2S,3S,4R,5S,6R)-4,5-Dihydroxy-6-[(2,2,2-trifluoro-acetylamino)-methyl]-2-((2R,3R,4S,5S,6S)-3,4,5-tris-benzyloxy-6-octyloxy-tetrahydro-pyran-2-ylmethoxy)-tetrahydro-pyran-3-yl]-2,2,2-trifluoro-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / sodium azide; 15-crown-5 / dimethylformamide / 60 °C

2.1: triphenylphosphine / tetrahydrofuran; H₂O / 20 °C

3.1: pyridine / 20 °C

3.2: 120 mg / methanol / 4 h / 20 °C

With pyridine; sodium azide; 15-crown-5; triphenylphosphine; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.11.063