pentyl phenylphosphonochloridate

Base Information

• Chemical Name: pentyl phenylphosphonochloridate
• CAS No.: 53121-76-9
• Molecular Formula: C₁₁H₁₆ClO₂P
• Molecular Weight: 246.674
• Mol file: 53121-76-9.mol

Synonyms:pentyl phenylphosphonochloridate

Chemical Property of pentyl phenylphosphonochloridate

Chemical Property:

Purity/Quality:

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Technology Process of pentyl phenylphosphonochloridate

There total 1 articles about pentyl phenylphosphonochloridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

P,P-dichlorophenylphosphine oxide (824-72-6) + pentan-1-ol (71-41-0) → pentyl phenylphosphonochloridate (53121-76-9)

Guidance literature:

With triethylamine; at 0 - 50 ℃;

DOI:10.1139/V10-111

Reference yield: 81.3%

pentyl phenylphosphonochloridate (53121-76-9) → O-pentyl phenylphosphorohydrazide

Guidance literature:

With hydrazine hydrate supported on basic alumina; at 0 - 60 ℃;

DOI:10.1139/V10-111

Reference yield: 43.7%

pentyl phenylphosphonochloridate (53121-76-9) + N-(4-hydroxybut-2-ynyl)anabasine → Phenyl-phosphonic acid 4-(1',2',3',4',5',6'-hexahydro-[2,3']bipyridinyl-6'-yl)-but-2-ynyl ester pentyl ester (145068-11-7)

Guidance literature:

With triethylamine; In diethyl ether; Heating;

DOI:10.1007/BF00629937

upstream raw materials:

P,P-dichlorophenylphosphine oxide

pentan-1-ol

Downstream raw materials:

N-β-hydroxypropylanabasinyl pentyl phenylphosphonate

Phenyl-phosphonic acid 4-(1',2',3',4',5',6'-hexahydro-[2,3']bipyridinyl-6'-yl)-but-2-ynyl ester pentyl ester