(S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde

Base Information

• Chemical Name: (S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde
• CAS No.: 76675-46-2
• Molecular Formula: C₁₅H₂₄O₂
• Molecular Weight: 236.354
• Mol file: 76675-46-2.mol

Synonyms:(S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde

Chemical Property of (S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde

There total 1 articles about (S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-3-buten-2-ol (115-18-4) + (S)-(-)-perillaldehyde (18031-40-8) → formiate de methyl-3 butene-2 ol-1 (68480-28-4) + hydroxydihydrolavandulol (95603-65-9,132311-99-0) + (S)-4-((R)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde (76675-48-4) + (S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde (76675-46-2)

Guidance literature:

With formic acid; hydrogen cation; Yield given. Multistep reaction; 1.) CH₂Cl₂, 20 min, 2.) MeOH, 2 h, 25 deg C;

DOI:10.1016/S0040-4039(00)77825-7

Reference yield:

(S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde (76675-46-2) → (-)-α-bisabolol (515-69-5,23089-26-1,23178-88-3,25428-43-7,72059-10-0,72691-24-8,76738-75-5,78148-59-1,123877-54-3,26560-22-5)

Guidance literature:

Multi-step reaction with 3 steps

1: LiAlH₄

2: pyridine

3: LiAlH₄

With pyridine; lithium aluminium tetrahydride;

DOI:10.1016/S0040-4039(00)77825-7

Reference yield:

(S)-4-((S)-1-Hydroxy-1,5-dimethyl-hex-4-enyl)-cyclohex-1-enecarbaldehyde (76675-46-2) → (S)-2-((S)-4-Hydroxymethyl-cyclohex-3-enyl)-6-methyl-hept-5-en-2-ol (116537-80-5)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1016/S0040-4039(00)77825-7

upstream raw materials:

2-methyl-3-buten-2-ol

(S)-(-)-perillaldehyde

Downstream raw materials:

(S)-2-((S)-4-Hydroxymethyl-cyclohex-3-enyl)-6-methyl-hept-5-en-2-ol

(-)-α-bisabolol