5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

Base Information

Chemical Name:5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole
CAS No.:1019321-19-7
Molecular Formula:C₁₅H₁₄Cl₂N₆O₃
Molecular Weight:397.221
Hs Code.:

Synonyms:5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

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Chemical Property of 5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

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Technology Process of 5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

There total 4 articles about 5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1019321-20-0
2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethoxy]benzoyl chloride

: 5203-77-0
1,3-dimethyl-1H-pyrazol-5-ol

: 1019321-19-7
5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

Guidance literature:: With triethylamine; In tetrahydrofuran; at 5 - 20 ℃; for 6h;

Reference yield:

: 579453-81-9
ethyl 2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethoxy]benzoate

: 1019321-19-7
5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium hydroxide; water / 7 h / 20 °C

2: thionyl chloride / N,N-dimethyl-formamide / 1,2-dichloro-ethane / 3 h / Heating / reflux

3: triethylamine / tetrahydrofuran / 6 h / 5 - 20 °C

With methanol; sodium hydroxide; thionyl chloride; water; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 130228-21-6
ethyl 2,4-dichloro-3-(2-bromo-ethoxy)-benzoate

: 1019321-19-7
5-{2,4-dichloro-3-[2-(1H-tetrazol-1-yl)ethyloxy]-benzoyloxy}-1,3-dimethylpyrazole

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 3 h / 80 °C

2: methanol; sodium hydroxide; water / 7 h / 20 °C

3: thionyl chloride / N,N-dimethyl-formamide / 1,2-dichloro-ethane / 3 h / Heating / reflux

4: triethylamine / tetrahydrofuran / 6 h / 5 - 20 °C

With methanol; sodium hydroxide; thionyl chloride; water; potassium carbonate; triethylamine; sodium iodide; N,N-dimethyl-formamide; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide;