1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

Base Information

Chemical Name:1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide
CAS No.:871508-38-2
Molecular Formula:C₂₇H₃₅N₅O₄
Molecular Weight:493.606
Hs Code.:

Synonyms:1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

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Technology Process of 1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

There total 1 articles about 1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 871508-36-0
N-Fmoc-Ac₆c-L-Asn-L-AllylGly-(1-naphthyl)methyl amide

: 871508-38-2
1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.666667h;

Reference yield: 65.0%

: (βR)-β-[[[4-[[bis(tert-butyloxy)phosphinyl]methyl]phenyl]-3-prop-2-enyl]amino]-butanedioic acid 1-mono(tert-butyl) ester

: 871508-38-2
1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

: 1-[[(βR)-β-[[[4-[[bis(tert-butyloxy)phosphinyl]methyl]phenyl]-3-prop-2-enyl]amino]-γ-(tert-butyl)butane-1,4-dioyl]amino]cyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 50 ℃; for 36h;
DOI:10.1021/jo701831q

Reference yield: 45.0%

: 871508-38-2
1-aminocyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

: (2S)-[(1S)-1-[4-[[bis(tert-butyloxy)phosphinyl]methyl]phenyl]-3-butenyl]-butanedioic acid 4-mono(tert-butyl) ester

: 1-[[(2S,3S)-3-[4-[[bis(tert-butyloxy)phosphinyl]methyl]phenyl]-2-[2-(tert-butyloxy)-2-oxoethyl]-1-oxo-5-hexenyl]amino]cyclohexanecarbonyl-L-asparaginyl-4,5-didehydro-N-(1-naphthalenylmethyl)-L-norvalinamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 50 ℃; for 36h;
DOI:10.1021/jo701831q