2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical

Base Information

• Chemical Name: 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical
• CAS No.: 1141880-21-8
• Molecular Formula: C₂₇H₂₀N₅O₁₀
• Molecular Weight: 574.483
• Mol file: 1141880-21-8.mol

Synonyms:2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical

Chemical Property of 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical

There total 2 articles about 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

2,2-diphenyl-1-(2,4,6-trinitrophenyl)hydrazyl (147506-92-1,1898-66-4) + C9H9O4(1-)*C10H20O5*Na(1+) → 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical (1141880-21-8) + 2-(p-nitrophenyl)-2-phenyl-1-(2,4,6-trinitrophenyl)hydrazine (29946-26-7) + 2,2-di(p-nitrophenyl)-1-(2,4,6-trinitrophenyl)hydrazine (5905-68-0)

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

DOI:10.1002/ejoc.200800735

Reference yield:

2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazine (1141880-22-9) → 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical (1141880-21-8)

Guidance literature:

With lead dioxide;

DOI:10.1002/ejoc.200800735

Reference yield: 98.0%

2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazyl radical (1141880-21-8) → 2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazine (1141880-22-9)

Guidance literature:

With ascorbic acid; In dichloromethane; water;

DOI:10.1002/ejoc.200800735

upstream raw materials:

2,2-diphenyl-1-(2,4,6-trinitrophenyl)hydrazyl

2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazine

Downstream raw materials:

2-[4-(4-formyl-2,6-dimethoxyphenoxy)phenyl]-2-phenyl-1-picrylhydrazine