cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)]

Base Information

• Chemical Name: cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)]
• CAS No.: 1371578-07-2
• Molecular Formula: C₆₉H₈₅N₁₁O₁₂
• Molecular Weight: 1260.5

Synonyms:cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)]

Chemical Property of cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)]

Chemical Property:

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Technology Process of cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)]

There total 1 articles about cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C33H43N7O9 (1203557-74-7) + C42H56N4O7 → cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)] (1371578-07-2)

Guidance literature:

C₃₃H₄₃N₇O₉; C₄₂H₅₆N₄O₇; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 10h;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Further stages;

DOI:10.1016/j.tet.2012.02.015

Reference yield: 93.4%

cyclo-[Orn(Nα-4''-octyloxy-terphenyl-4-formyl)-Thr-Pro-hTyr-Orn(Nδ-Cbz)-Pro(4S-N3)] (1371578-07-2) + toluene-4-sulfonic acid (104-15-4) → 2C7H8O3S*C61H81N9O10

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2012.02.015

upstream raw materials:

C₃₃H₄₃N₇O₉

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