ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate

Base Information

Chemical Name:ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate
CAS No.:1080060-30-5
Molecular Formula:C₂₁H₂₈O₆S
Molecular Weight:408.516
Hs Code.:

Synonyms:ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate

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Chemical Property of ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate

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Technology Process of ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate

There total 1 articles about ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 745052-93-1
2-[4-(cyclopropylsulfonyl)phenyl]-3-(tetrahydro-2H-pyran-4-yl)propionic acid

: 6148-64-7
ethyl potassium malonate

: 1080060-30-5
ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate

Guidance literature:: 2-[4-(cyclopropylsulfonyl)phenyl]-3-(tetrahydro-2H-pyran-4-yl)propionic acid; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

ethyl potassium malonate; With magnesium chloride; In tetrahydrofuran; at 60 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield: 24.0%

: 3292-77-1
2-bromo-1-thiazol-2-yl-ethanone

: 1080060-30-5
ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate

: 1080060-31-6
ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-2-[2-oxo-2-(1,3-thiazol-2-yl)ethyl]-5-(tetrahydro-2H-pyran-4-yl)pentanoate

Guidance literature:: ethyl 4-[4-(cyclopropylsulfonyl)phenyl]-3-oxo-5-(tetrahydro-2H-pyran-4-yl)pentanoate; With sodium hydride; In tetrahydrofuran; oil; at 0 ℃; for 0.25h; Inert atmosphere;

2-bromo-1-thiazol-2-yl-ethanone; In tetrahydrofuran; oil; at 0 - 20 ℃;

With water; ammonium chloride; In tetrahydrofuran; oil;