Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

Base Information

• Chemical Name: Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆
• CAS No.: 87114-73-6
• Molecular Formula: C₃₄H₄₄ClFeN₆*F₆P
• Molecular Weight: 773.028

Synonyms:Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

Chemical Property of Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆

There total 1 articles about Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe⁽¹⁺⁾*PF₆^(1-)=(Cl(CH₂)4(NCH₃CC₆H₅C₃HCH₃N₂(CH₂)3)2Fe)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Fe(py)2Cl2 (15616-26-9) + H4(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2(4+)*3PF6(1-)*Cl(1-)=(H4(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2)(PF6)3Cl → Cl(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2Fe(1+)*PF6(1-)=(Cl(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2Fe)PF6 (87114-73-6)

Guidance literature:

With triethylamine; In acetonitrile; ligand and slight excess of Fe complex slurring in MeCN; large excess of Et3N adding, refluxing for 5 min, cooling and filtering through celite, solvent removing, residue dissolving in hot MeOH, stirring for 10 min,filtering; purified by recrystn. from MeCN/EtOH or MeOH; identified by elem. anal.;

DOI:10.1021/ja00360a008

Reference yield:

Cl(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2Fe(1+)*PF6(1-)=(Cl(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2Fe)PF6 (87114-73-6) → Cl(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2Fe(2+)*2PF6(1-)=(Cl(CH2)4(NCH3CC6H5C3HCH3N2(CH2)3)2Fe)(PF6)2

Guidance literature:

With O₂; In acetone; exposure to O2 at 254 K; Kinetics;

DOI:10.1021/ja00360a008

upstream raw materials:

Fe(py)2Cl₂

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