5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

Base Information

Chemical Name:5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide
CAS No.:99519-83-2
Molecular Formula:C₁₇H₁₃Cl₂N₅O₂
Molecular Weight:390.229
Hs Code.:

Synonyms:5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

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Chemical Property of 5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

Chemical Property:

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Technology Process of 5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

There total 5 articles about 5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99519-99-0
4-(4-chlorobenzoyl)-3-chlorobenzyl azide

: 107-91-5
cyanoacetic acid amide

: 99519-83-2
5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

Guidance literature:: With sodium methylate; Yield given. Multistep reaction; 1.) EtOH, reflux, 20 min, 2.) EtOH, reflux, 2 h;

Reference yield:

: 7697-25-8
2-chloro-4-methylbenzoic acid

: 99519-83-2
5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: SOCl₂, DMF / 3 h / Heating

2: AlCl₃ / 15 h / 85 °C

3: 45.1 percent / dibenzoyl peroxide, NBS / benzene / 23 h / Heating

4: NaN₃ / ethanol / 5 h / Heating

5: 1.) NaOCH₃ / 1.) EtOH, reflux, 20 min, 2.) EtOH, reflux, 2 h

With N-Bromosuccinimide; aluminium trichloride; thionyl chloride; sodium azide; sodium methylate; N,N-dimethyl-formamide; dibenzoyl peroxide; In ethanol; benzene;

Reference yield:

: 21900-53-8
2-chloro-4-methyl-benzoyl chloride

: 99519-83-2
5-amino-1-(4-[4-chlorobenzoyl]-3-chlorobenzyl)-1,2,3-triazole-4-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: AlCl₃ / 15 h / 85 °C

2: 45.1 percent / dibenzoyl peroxide, NBS / benzene / 23 h / Heating

3: NaN₃ / ethanol / 5 h / Heating

4: 1.) NaOCH₃ / 1.) EtOH, reflux, 20 min, 2.) EtOH, reflux, 2 h

With N-Bromosuccinimide; aluminium trichloride; sodium azide; sodium methylate; dibenzoyl peroxide; In ethanol; benzene;