Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid

Base Information

• Chemical Name: Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid
• CAS No.: 75809-93-7
• Molecular Formula: C₃₆H₃₅Br₂IO₁₁S₂
• Molecular Weight: 994.512

Synonyms:Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid

Chemical Property of Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid

Chemical Property:

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Technology Process of Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid

There total 3 articles about Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

Methyl-3-O-<3-O-benzoyl-4,6-O-benzyliden-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-4,6-O-benzyliden-2-desoxy-2-iod-α-D-mannopyranosid → Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid (75809-93-7)

Guidance literature:

With N-Bromosuccinimide; barium carbonate; dibenzoyl peroxide; In benzene; at 90 ℃; for 1h;

DOI:10.1002/cber.19801130918

Reference yield:

1-benzoylimidazole (10364-94-0) → Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid (75809-93-7)

Guidance literature:

Multi-step reaction with 2 steps

2: 40 percent / BaCO₃, NBS, dibenzoyl peroxide / benzene / 1 h / 90 °C

With N-Bromosuccinimide; barium carbonate; dibenzoyl peroxide; In benzene;

DOI:10.1002/cber.19801130918

Reference yield:

(2R,4aR,6S,7R,8R,8aS)-6-((2R,4aR,6S,7S,8S,8aR)-7-Iodo-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol → Methyl-4-O-benzoyl-6-brom-2,6-didesoxy-3-O-<3,4-di-O-benzoyl-6-brom-6-desoxy-2-O-<(methylthio)thiocarbonyl>-β-D-glucopyranosyl>-2-iod-α-D-mannopyranosid (75809-93-7)

Guidance literature:

Multi-step reaction with 2 steps

2: 40 percent / BaCO₃, NBS, dibenzoyl peroxide / benzene / 1 h / 90 °C

With N-Bromosuccinimide; barium carbonate; dibenzoyl peroxide; In benzene;

DOI:10.1002/cber.19801130918

upstream raw materials:

1-benzoylimidazole

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