bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2]

Base Information

• Chemical Name: bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2]
• CAS No.: 105332-54-5
• Molecular Formula: C₆NiS₁₀*C₃₆H₃₀NP₂
• Molecular Weight: 990.004

Synonyms:bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2]

Chemical Property of bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2]

Chemical Property:

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Technology Process of bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2]

There total 1 articles about bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

[bis(triphenylphosphoranylidene)ammonium]2[Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2] → bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2] (105332-54-5)

Guidance literature:

With air; In acetone; bubbling air for 30 min; vol. reduction (reduced pressure), pptn. on MeOH addn., collection (filtration), drying (vac.); elem. anal.;

DOI:10.1016/S0277-5387(97)00131-9

Reference yield: 28.0%

bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2] (105332-54-5) + iodine (7553-56-2,12190-71-5,8031-47-8) → [bis(triphenylphosphine)iminium]0.25[Ni(1,3-dithiole-2-thione-4,5-dithiolate)2]

Guidance literature:

In acetonitrile; N2-atmosphere; equimolar amts.; pptn. on cooling overnight; elem. anal.;

DOI:10.1016/S0277-5387(97)00131-9

Reference yield:

bis(triphenylphosphoranylidene)ammonium [Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2] (105332-54-5) → [bis(triphenylphosphoranylidene)ammonium]2[Ni(2-thioxo-1,3-dithiole-4,5-dithiolato)2]3

Guidance literature:

In not given; Electrochem. Process; galvanostatic oxidation according to Cassoux, P. et al.: Inorganic Materials; Bruce, D. W. et al. (Eds.), Wiley, Chichester 1992, pp. 1-58;

DOI:10.1021/ic9600341

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