{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

Base Information

Chemical Name:{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid
CAS No.:1064662-90-3
Molecular Formula:C₁₈H₁₈N₂O₆
Molecular Weight:358.351
Hs Code.:

Synonyms:{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

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Chemical Property of {(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

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Technology Process of {(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

There total 1 articles about {(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1064662-87-8
{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid hydrochloride

: 1064662-90-3
{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

Guidance literature:: With sodium hydroxide; In water; for 1h;

Reference yield: 61.0%

: 1064662-90-3
{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

: 104-15-4
toluene-4-sulfonic acid

: 1064662-91-4
(2S)-2-[(benzylamino)methyl]-2,3,8,9-tetrahydro-7H-[1,4]dioxino[2,3-e]indol-8-one 4-methylbenzenesulfonate

Guidance literature:: With hydrogen; platinum on carbon; In methanol; for 18h;

Reference yield:

: 1064662-90-3
{(3S)-3-[(benzylamino)methyl]-6-nitro-2,3-dihydro-1,4-benzodioxin-5-yl}acetic acid

: 189681-71-8
Aplindore fumarate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / platinum on carbon / methanol / 18 h

2.1: sodium hydroxide / 2-methyltetrahydrofuran; water / pH 10

2.2: 75 - 80 °C / Inert atmosphere

With hydrogen; sodium hydroxide; platinum on carbon; In 2-methyltetrahydrofuran; methanol; water;