6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester
CAS No.:178265-90-2
Molecular Formula:C₂₆H₂₂ClNO₃
Molecular Weight:431.919
Hs Code.:

Synonyms:6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

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Chemical Property of 6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

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Technology Process of 6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

There total 1 articles about 6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 178265-89-9
4-(4-Chloro-phenyl)-3,6-dihydro-2H-pyridine-1-carboxylic acid 9H-fluoren-9-ylmethyl ester

: 178265-90-2
6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 18h;
DOI:10.1021/ja954069w

Reference yield:

: 178265-90-2
6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

: 6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h;
DOI:10.1021/ja954069w

Reference yield:

: 178265-90-2
6-(4-Chloro-phenyl)-7-oxa-3-aza-bicyclo[4.1.0]heptane-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

: N-(4-p-fluorophenyl-4-oxobutyl)-4-(p-chlorophenyl)-3,4-epoxypiperidine

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / dimethylformamide / 0.5 h / 25 °C

2: K₂CO₃ / dimethylformamide / 0.5 h / Heating

With piperidine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ja954069w