(S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

Base Information

Chemical Name:(S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester
CAS No.:204916-68-7
Molecular Formula:C₁₉H₂₂O₄
Molecular Weight:314.381
Hs Code.:

Synonyms:(S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

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Chemical Property of (S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

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Technology Process of (S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

There total 6 articles about (S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-Methoxy-phenyl-acetic acid 2-(2-hydroxy-4-methyl-cyclohex-3-enyl)-allyl ester

: 204916-68-7
(S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

: 204916-67-6
(S)-Methoxy-phenyl-acetic acid 2-((S)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 ℃; for 2h; Yield given. Yields of byproduct given;

Reference yield:

: 52062-24-5
(E)-1-acetoxy-3-methyl-1,3-butadiene

: 204916-68-7
(S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / benzene / 8.5 h / Heating

2: 80 percent / BuLi / tetrahydrofuran; hexane / Ambient temperature

3: 74 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

4: 87 percent / DCC / CH₂Cl₂ / Ambient temperature

5: triacetoxyperiodinane (Dess-Martin) / CH₂Cl₂ / 2 h / 0 °C

With lithium aluminium tetrahydride; n-butyllithium; Dess-Martin periodane; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; benzene;

Reference yield:

: 26164-26-1
(S)-2-methoxy-2-phenylacetic acid

: 204916-68-7
(S)-Methoxy-phenyl-acetic acid 2-((R)-4-methyl-2-oxo-cyclohex-3-enyl)-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DCC / CH₂Cl₂ / Ambient temperature

2: triacetoxyperiodinane (Dess-Martin) / CH₂Cl₂ / 2 h / 0 °C

With Dess-Martin periodane; dicyclohexyl-carbodiimide; In dichloromethane;