dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate

Base Information

• Chemical Name: dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate
• CAS No.: 220230-84-2
• Molecular Formula: C₄₃H₃₇NO₈
• Molecular Weight: 695.769

Synonyms:dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate

Chemical Property of dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate

Chemical Property:

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Technology Process of dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate

There total 6 articles about dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-Bromo-4'-methoxyacetophenone (2632-13-5) + dimethyl 3,4-bis(4-(benzyloxy)phenyl)-1H-pyrrole-2,5-dicarboxylate (220230-81-9) → dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate (220230-84-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

DOI:10.1021/ja982078+

Reference yield:

1,2,4,5-tetrazine-3,6-dicarboxylic acid dimethyl ester (2166-14-5) → dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate (220230-84-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / toluene / 72 h / 110 °C

2: 72 percent / Zn, AcOH / 18 h / 25 °C

3: 100 percent / K₂CO₃ / dimethylformamide / 1 h / 70 °C

With potassium carbonate; acetic acid; zinc; In N,N-dimethyl-formamide; toluene;

DOI:10.1021/ja982078+

Reference yield:

1,2-bis(4-benzyloxyphenyl)acetylene (16819-41-3) → dimethyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2,5-dicarboxylate (220230-84-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / toluene / 72 h / 110 °C

2: 72 percent / Zn, AcOH / 18 h / 25 °C

3: 100 percent / K₂CO₃ / dimethylformamide / 1 h / 70 °C

With potassium carbonate; acetic acid; zinc; In N,N-dimethyl-formamide; toluene;

DOI:10.1021/ja982078+

upstream raw materials:

2-Bromo-4'-methoxyacetophenone

dimethyl 3,4-bis(4-(benzyloxy)phenyl)-1H-pyrrole-2,5-dicarboxylate

1,2,4,5-tetrazine-3,6-dicarboxylic acid dimethyl ester

1,2-bis(4-benzyloxyphenyl)acetylene

Downstream raw materials:

methyl 3,4-bis(4-benzyloxyphenyl)-1-<2-(4-methoxyphenyl)-2-oxoethyl>pyrrole-2-carboxylate

3,4-bis-(4-benzyloxy-phenyl)-1-[2-(4-methoxy-phenyl)-2-oxo-ethyl]-1H-pyrrole-2-carboxylic acid

1H-7,8-bis(4-benzyloxyphenyl)-3-(methoxyphenyl)pyrrolo<2,1-c><1,4>-oxazin-1-one

3,7,8-tris(4-hydroxyphenyl)-1H-pyrrolo[2,1-c][1,4]oxazin-1-one

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