decamethylscandocene*BPh₄

Base Information

Chemical Name:decamethylscandocene*BPh₄
CAS No.:869648-30-6
Molecular Formula:C₂₀H₃₀Sc*C₂₄H₂₀B
Molecular Weight:634.648
Hs Code.:

Synonyms:decamethylscandocene*BPh₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of decamethylscandocene*BPh₄

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Technology Process of decamethylscandocene*BPh₄

There total 1 articles about decamethylscandocene*BPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 99707-15-0
(eta.5-C₅Me₅)2ScCH₃

: N,N-dimethylanilinium tetraphenylborate

: 869648-30-6
decamethylscandocene*BPh₄

Guidance literature:: In toluene; byproducts: CH4, (C6H5)N(CH3)2; (Schlenk; N2 atm.) toluene was added to a mixt. of complexes, 1 h; the solvent was evapd., the solid was washed with pentane; elem. anal.;
DOI:10.1021/ja054544i

Reference yield: 62.0%

: 869648-30-6
decamethylscandocene*BPh₄

: N,N'-dimethylaniliniumtetrakis(pentafluorophenyl)borate

: 869648-50-0
[(η5-C5Me5)2Sc(κ2-F-C6F5)B(C6F5)3]

Guidance literature:: In toluene; (Schlenk; N2 atm.) toluene was added to the mixt. of coomplexes; layered with cyclohexane for one week, decanted, washed with pentane; elem. anal.;
DOI:10.1021/ja054544i

Reference yield: 44.0%

: 869648-30-6
decamethylscandocene*BPh₄

: 367-11-3
ortho-difluorobenzene

: 869648-42-0
[(η5-C5Me5)2Sc(κ2-F-1,2-difluorobenzene)][BPh4]

Guidance literature:: In neat (no solvent); (Schlenk; N2 atm.) 1,2-difluorobenzene was added to complex; cyclohexane was layered carefully, elem. anal.;
DOI:10.1021/ja054544i