(5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

Base Information

Chemical Name:(5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide
CAS No.:123472-52-6
Molecular Formula:C₃₆H₄₄N₄O₇S₃
Molecular Weight:740.966
Hs Code.:

Synonyms:(5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

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Technology Process of (5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

There total 9 articles about (5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 124659-27-4
(5S)-N-(5,9-diamino-7-azanonyl)benzamide

: 98-59-9
p-toluenesulfonyl chloride

: 123472-52-6
(5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

Guidance literature:: With triethylamine; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1039/P19900002567

Reference yield:

: 124659-25-2
(2S)-N-(2-aminoethyl)-2,6-diaminohexanamide

: 123472-52-6
(5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / BH₃ / tetrahydrofuran / 21 h / 70 °C

3: 63 percent / Et₃N / CH₂Cl₂

With borane; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39890000794

Reference yield:

: 124659-26-3
(5S)-3-azanonane-1,5,9-triamine

: 123472-52-6
(5S)-N-(5,9-bistoluene-p-sulphonamino-7-toluene-p-sulphonyl-7-azanonyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

2: 63 percent / Et₃N / CH₂Cl₂

With triethylamine; In dichloromethane;
DOI:10.1039/c39890000794