bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

Base Information

Chemical Name:bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide
CAS No.:1385144-79-5
Molecular Formula:C₄₄H₆₆Cl₂N₆O₁₀
Molecular Weight:909.948
Hs Code.:

Synonyms:bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

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Chemical Property of bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

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Technology Process of bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

There total 3 articles about bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 124-09-4
1,6-Hexanediamine

: 78841-25-5
N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine pentafluorophenyl ester

: 1385144-79-5
bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

Guidance literature:: In ethyl acetate; for 1h;

Reference yield: 85.0%

: 124-09-4
1,6-Hexanediamine

: 66438-39-9
N^α-Boc-N^ε-(2-Cl-Cbz)-L-lysine N-hydroxysuccinimide ester

: 1385144-79-5
bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

Guidance literature:: In ethyl acetate; for 1h;
DOI:10.1134/S1068162012030053

Reference yield:

: 54613-99-9
Boc-(S)-Lys(2-Cl-Z)-OH

: 1385144-79-5
bis-(N-t-butyloxycarbonyl-Nε-(2-chlorobenzyloxycarbonyl)lysine)hexamethylenediamide

Guidance literature:: Multi-step reaction with 2 steps

1: dicyclohexyl-carbodiimide / tetrahydrofuran / 5 h / -5 - 20 °C

2: ethyl acetate / 1 h

With dicyclohexyl-carbodiimide; In tetrahydrofuran; ethyl acetate;
DOI:10.1134/S1068162012030053