<α-2H>acrylophenone

Base Information

• Chemical Name: <α-2H>acrylophenone
• CAS No.: 147991-75-1
• Molecular Formula: C₉H₈O
• Molecular Weight: 133.154

Synonyms:<α-2H>acrylophenone

Chemical Property of <α-2H>acrylophenone

Chemical Property:

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Technology Process of <α-2H>acrylophenone

There total 6 articles about <α-2H>acrylophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

(R)-(-)-<2,2-2H2>-1-phenylcyclopropylamine hydrochloride → <α-2H>acrylophenone (147991-75-1) + <β,β-2H2>acrylophenone + Phenyl vinyl ketone (768-03-6,26742-84-7)

Guidance literature:

With monoamine oxidase-B (MAO-B); NaPi buffer; at 25 ℃; Product distribution; Mechanism; other labeled and unlabeled 1-phenylcyclopropylamines;

DOI:10.1021/ja00065a002

Reference yield:

1-phenyl-1-deuterium-prop-2-yn-1-ol → <α-2H>acrylophenone (147991-75-1) + Phenyl vinyl ketone (768-03-6,26742-84-7)

Guidance literature:

With [Ph₄(η₄-2,3,4,5-tetraphenylcyclopentadienone)]Ru⁰(CO)₃; trifluoroacetic acid; In benzene-d6; at 80 ℃; for 8h; regioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201200188

Reference yield:

1-phenyl-1-deuterium-prop-2-yn-1-ol → α-deuteriostyrene (1193-80-2) + cinnamaldehyde-3-d (17537-29-0) + <α-2H>acrylophenone (147991-75-1) + Phenyl vinyl ketone (768-03-6,26742-84-7)

Guidance literature:

With C₂₄H₂₀N₂O₄Ru; trifluoroacetic acid; In benzene-d6; at 80 ℃; for 8h; regioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201200188

upstream raw materials:

C₁₂H₁₆⁽²⁾H₂NO⁽¹⁺⁾*Br^(1-)

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