C₂₈H₄₇N₃O₇Si

Base Information

Chemical Name:C₂₈H₄₇N₃O₇Si
CAS No.:1426657-17-1
Molecular Formula:C₂₈H₄₇N₃O₇Si
Molecular Weight:565.783
Hs Code.:

C<sub>28</sub>H<sub>47</sub>N<sub>3</sub>O<sub>7</sub>Si

Synonyms:C₂₈H₄₇N₃O₇Si

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Chemical Property of C₂₈H₄₇N₃O₇Si

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Technology Process of C₂₈H₄₇N₃O₇Si

There total 9 articles about C₂₈H₄₇N₃O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1426656-67-8
C₃₄H₆₁N₃O₇Si₂

: 1426657-17-1
C₂₈H₄₇N₃O₇Si

Guidance literature:: With (1S)-10-camphorsulfonic acid; In methanol; dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c3cc00178d

Reference yield:

: 159718-22-6
(2R,3R)-(+)-2-azido-3-isopropyl-3-hydroxypropionic acid

: 1426657-17-1
C₂₈H₄₇N₃O₇Si

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C / Inert atmosphere

2: silver cyanide / toluene / 1 h / 0 - 80 °C / Inert atmosphere

3: triphenylphosphine / tetrahydrofuran; water / 18 h / Inert atmosphere; Reflux

4: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5: (1S)-10-camphorsulfonic acid / dichloromethane; methanol / 2 h / 0 - 20 °C / Inert atmosphere

With silver cyanide; oxalyl dichloride; (1S)-10-camphorsulfonic acid; triethylamine; N,N-dimethyl-formamide; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1039/c3cc00178d

Reference yield:

: 159990-09-7
(2R,3R)-(+)-ethyl 2-azido-3-isopropyl-3-hydroxypropionate

: 1426657-17-1
C₂₈H₄₇N₃O₇Si

Guidance literature:: Multi-step reaction with 6 steps

1: lithium hydroxide; water / methanol; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0 °C / Inert atmosphere

3: silver cyanide / toluene / 1 h / 0 - 80 °C / Inert atmosphere

4: triphenylphosphine / tetrahydrofuran; water / 18 h / Inert atmosphere; Reflux

5: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

6: (1S)-10-camphorsulfonic acid / dichloromethane; methanol / 2 h / 0 - 20 °C / Inert atmosphere

With silver cyanide; oxalyl dichloride; (1S)-10-camphorsulfonic acid; water; triethylamine; N,N-dimethyl-formamide; triphenylphosphine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1039/c3cc00178d