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Technology Process of N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

Base Information
  • Chemical Name:N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide
  • CAS No.:680227-99-0
  • Molecular Formula:C26H21Cl2F2N3O3S
  • Molecular Weight:564.44
  • Hs Code.:
N<sub>1</sub>-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N<sub>2</sub>-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

Synonyms:N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

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Chemical Property of N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide
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Technology Process of N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

There total 1 articles about N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,3-cis)-3-amino-2-(3,4-dichlorophenyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one hydrobromide

(2,3-cis)-3-amino-2-(3,4-dichlorophenyl)-2,3-dihydro-1,5-benzothiazepin-4(5H)-one hydrobromide

N-(3,5-Difluorophenylacetyl)-L-alanine
208124-34-9

N-(3,5-Difluorophenylacetyl)-L-alanine

N<sub>1</sub>-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N<sub>2</sub>-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide
680227-99-0

N1-[(2R,3R)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

N<sub>1</sub>-[(2S,3S)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N<sub>2</sub>-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

N1-[(2S,3S)-2-(3,4-dichlorophenyl)-4-oxo-2,3,4,5-tetrahydro-1,5-benzothiazepin-3-yl]-N2-[(3,5-difluoro-phenyl)acetyl]-L-alaninamide

Guidance literature:
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 2.5h;
upstream raw materials:

N-(3,5-Difluorophenylacetyl)-L-alanine

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