C₂₈H₂₉ClO₁₀

Base Information

Chemical Name:C₂₈H₂₉ClO₁₀
CAS No.:1327165-99-0
Molecular Formula:C₂₈H₂₉ClO₁₀
Molecular Weight:560.985
Hs Code.:

C<sub>28</sub>H<sub>29</sub>ClO<sub>10</sub>

Synonyms:C₂₈H₂₉ClO₁₀

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Chemical Property of C₂₈H₂₉ClO₁₀

Chemical Property:

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Technology Process of C₂₈H₂₉ClO₁₀

There total 12 articles about C₂₈H₂₉ClO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1185339-52-9
C₂₉H₃₁ClO₉

: 1327165-99-0
C₂₈H₂₉ClO₁₀

Guidance literature:: C₂₉H₃₁ClO₉; With ozone; In dichloromethane;

With triphenylphosphine; at -78 - 20 ℃;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 1185339-44-9
C₁₉H₂₁ClO₅

: 1327165-99-0
C₂₈H₂₉ClO₁₀

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap / pyridine; dichloromethane / 20 °C

2.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

4.1: toluene-4-sulfonic acid / water; toluene / Reflux

5.1: ozone / dichloromethane

5.2: -78 - 20 °C

With dmap; aluminum (III) chloride; sodium tetrahydroborate; toluene-4-sulfonic acid; ozone; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; toluene; 2.1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032

Reference yield:

: 312749-31-8
2-chloro-5-bromobenzophenone

: 1327165-99-0
C₂₈H₂₉ClO₁₀

Guidance literature:: Multi-step reaction with 9 steps

1.1: triethylsilane; trifluorormethanesulfonic acid; trifluoroacetic acid / Reflux

2.1: n-butyllithium / tetrahydrofuran; toluene / -78 °C

3.1: methanesulfonic acid / methanesulfonic acid / -78 - 20 °C

4.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / -30 - -10 °C

5.1: dmap / pyridine; dichloromethane / 20 °C

6.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C

7.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

8.1: toluene-4-sulfonic acid / water; toluene / Reflux

9.1: ozone / dichloromethane

9.2: -78 - 20 °C

With triethylsilane; dmap; aluminum (III) chloride; sodium tetrahydroborate; n-butyllithium; methanesulfonic acid; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; toluene-4-sulfonic acid; ozone; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; methanesulfonic acid; dichloromethane; water; toluene; acetonitrile; 6.1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2011.06.032