tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane

Base Information

• Chemical Name: tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane
• CAS No.: 203172-28-5
• Molecular Formula: C₂₇H₃₈O₄Si
• Molecular Weight: 454.682

Synonyms:tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane

Chemical Property of tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane

Chemical Property:

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Technology Process of tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane

There total 24 articles about tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-Butyl-((2S,5R,6R)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane (203172-29-6) → tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane (203172-28-5)

Guidance literature:

With hydrogenchloride; acetic acid; for 2h; Ambient temperature;

DOI:10.1016/0040-4039(96)01265-8

Reference yield: 97.0%

tert-Butyl-((2S,5R,6R,11R)-11-iodo-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane (203172-30-9) → tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane (203172-28-5)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 0.583333h; Heating;

DOI:10.1021/jo972023a

Reference yield: 80.0%

tert-Butyl-((2S,5R,6R,11S)-11-iodo-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane (203172-31-0) → tert-Butyl-((2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane (203172-28-5)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 0.583333h; Heating;

DOI:10.1021/jo972023a

upstream raw materials:

4-[(2R,3R,6S)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methoxy-tetrahydro-pyran-2-yl]-butan-1-ol

tert-Butyl-((2S,5R,6R)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane

4-[(2S,3R,6S)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-3-methoxy-tetrahydro-pyran-2-yl]-butan-1-ol

tert-Butyl-((2S,5R,6R,11R)-11-iodo-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethoxy)-diphenyl-silane

Downstream raw materials:

Toluene-4-sulfonic acid (2S,5R,6S)-5-methoxy-1,7-dioxa-spiro[5.5]undec-2-ylmethyl ester

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