Technology Process of 4-nitrobenzyl mercaptoacetylglycylglycylglycinate
There total 8 articles about 4-nitrobenzyl mercaptoacetylglycylglycylglycinate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chlorotriisopropylsilane; water; ethylene glycol; trifluoroacetic acid;
for 2h;
DOI:10.1016/j.bmcl.2011.10.022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 20 °C
2: 3 h / 20 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
4: chlorotriisopropylsilane; water; ethylene glycol; trifluoroacetic acid / 2 h
With
chlorotriisopropylsilane; water; benzotriazol-1-ol; ethylene glycol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C
2: chlorotriisopropylsilane; water; ethylene glycol; trifluoroacetic acid / 2 h
With
chlorotriisopropylsilane; water; benzotriazol-1-ol; ethylene glycol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.022
