5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

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Chemical Name:5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione
CAS No.:102212-79-3
Molecular Formula:C₂₃H₂₅N₅O₅S
Molecular Weight:483.548
Hs Code.:

Synonyms:5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

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Chemical Property of 5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

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Technology Process of 5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

There total 5 articles about 5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 102212-78-2
5-Hydroxy-1,3-dimethyl-6-(3-methyl-but-2-enyl)-8-(4-methylsulfanyl-benzyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

: 102212-79-3
5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 6h; Heating;
DOI:10.1021/jm00156a032

Reference yield:

: 22539-80-6
diethyl (3-methylbut-2-enyl)malonate

: 102212-79-3
5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) DMF, RT, 0.5 h, 2.) DMF, reflux, 18 h

2: 63 percent / m-chloroperbenzoic acid / CHCl₃ / 6 h / Heating

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1021/jm00156a032

Reference yield:

: 83171-39-5
4-(methylthio)benzylamine

: 102212-79-3
5-Hydroxy-8-(4-methanesulfinyl-benzyl)-1,3-dimethyl-6-(3-methyl-but-2-enyl)-1H,8H-1,3,4b,8,9-pentaaza-fluorene-2,4,7-trione

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 4 h / Heating

2: 1.) sodium hydride / 1.) DMF, RT, 0.5 h, 2.) DMF, reflux, 18 h

3: 63 percent / m-chloroperbenzoic acid / CHCl₃ / 6 h / Heating

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In chloroform;
DOI:10.1021/jm00156a032