1'-(1-cyclohexenyl)biferrocene

Base Information

• Chemical Name: 1'-(1-cyclohexenyl)biferrocene
• CAS No.: 1448254-62-3
• Molecular Formula: C₂₆H₂₆Fe₂
• Molecular Weight: 450.186
• Mol file: 1448254-62-3.mol

Synonyms:1'-(1-cyclohexenyl)biferrocene

Chemical Property of 1'-(1-cyclohexenyl)biferrocene

Chemical Property:

Purity/Quality:

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Technology Process of 1'-(1-cyclohexenyl)biferrocene

There total 1 articles about 1'-(1-cyclohexenyl)biferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1',1'''-bis(1-hydroxycyclohexyl)biferrocene (1448254-85-0) + 1'-(1-hydroxycyclohexyl)biferrocene (1448254-87-2) → 1,1''-biferrocene + 1',1'''-di-1-cyclohexenylbiferrocene (1448254-73-6) + 1'-(1-cyclohexenyl)biferrocene (1448254-62-3)

Guidance literature:

With toluene-4-sulfonic acid; at 110 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.05.041

Reference yield: 76.0%

1'-(1-cyclohexenyl)biferrocene (1448254-62-3) → 1'-cyclohexylbiferrocene (1448254-65-6)

Guidance literature:

With palladium on activated charcoal; hydrogen; In ethanol; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.05.041

Reference yield: 40.0%

1'-(1-cyclohexenyl)biferrocene (1448254-62-3) + [Fe(C5H4Br)2][Ni(maleonitriledithiolate)2] → C26H26Fe2*C8N4NiS4(2-)

Guidance literature:

In dichloromethane; acetone; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.jorganchem.2013.05.041

upstream raw materials:

1',1'''-bis(1-hydroxycyclohexyl)biferrocene

1'-(1-hydroxycyclohexyl)biferrocene

Downstream raw materials:

1'-cyclohexylbiferrocene