ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

Base Information

Chemical Name:ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate
CAS No.:1163128-90-2
Molecular Formula:C₂₀H₃₄Cl₂NO₅PS
Molecular Weight:502.439
Hs Code.:

Synonyms:ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

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Chemical Property of ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

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Technology Process of ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

There total 1 articles about ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 844646-94-2
(S)-N-(2,4-dichlorophenyl)methylene-2-methylpropane-2-sulfinamide

: 75174-69-5
1-[1-ethoxy-1-(ethoxy(methyl)phosphoryl)ethoxy]ethane

: 1163128-90-2
ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

: 1163128-91-3
ethyl 1',1'-diethoxyethyl-(S(S),R(C),R(P))-(-)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

Guidance literature:: 1-[1-ethoxy-1-(ethoxy(methyl)phosphoryl)ethoxy]ethane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

(S)-N-(2,4-dichlorophenyl)methylene-2-methylpropane-2-sulfinamide; In tetrahydrofuran; at -78 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200802248

Reference yield: 82.0%

: 1163128-90-2
ethyl 1',1'-diethoxyethyl-(S(S),R(C),S(P))-(+)-2-(tert-butylsulfinylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

: 1163128-94-6
ethyl 1',1'-diethoxyethyl-(R(C),S(P))-(-)-2-(tert-butylsulfonylamino)-2-(2,4-dichlorophenyl)ethylphosphinate

Guidance literature:: With sodium periodate; ruthenium(III) trichloride hydrate; In dichloromethane; water; acetonitrile; at 20 ℃; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/chem.200802248