((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))PF₆

Base Information

• Chemical Name: ((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))PF₆
• CAS No.: 896732-86-8
• Molecular Formula: C₂₁H₃₀FeN₂O₃P*F₆P
• Molecular Weight: 590.266

Synonyms:((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))PF₆

Chemical Property of ((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))PF₆

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Technology Process of ((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))PF₆

There total 1 articles about ((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))⁽¹⁺⁾*PF₆^(1-)=((C₅(CH₃)5)Fe(CO)(CH₃CN)(P(OCH₃)2NHC₆H₅))PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

[(η5-pentamethylcyclopentadienyl)Fe(CO)2(acetonitrile)][PF6] + P(N(SiMe3)Ph)(OMe)2 (433217-88-0) → ((C5(CH3)5)Fe(CO)(CH3CN)(P(OCH3)2NHC6H5))(1+)*PF6(1-)=((C5(CH3)5)Fe(CO)(CH3CN)(P(OCH3)2NHC6H5))PF6 (896732-86-8)

Guidance literature:

In dichloromethane; Irradiation (UV/VIS); under N2 atm. soln. Fe complex in MeCN was irradiated with UV light for 1 h at 0°C, volatiles were removed in vacuo, residue was washed with ether and dissolved in CH2Cl2, P(N(SiMe3)Ph)(OMe)2 was added and refluxed overnight; soln. was evapd. to dryness, residue was dissolved in aq. THF and stirred at 45°C for 45°C, volatiles were removed in vacuo, residue was dissolved in CH2Cl2 and chromed. on silica (CH2Cl2-acetone 9:1), soln. was dried in vacuo; elem. anal.;

DOI:10.1021/om0510728

Reference yield: 77.0%

((C5(CH3)5)Fe(CO)(CH3CN)(P(OCH3)2NHC6H5))(1+)*PF6(1-)=((C5(CH3)5)Fe(CO)(CH3CN)(P(OCH3)2NHC6H5))PF6 (896732-86-8) → [Cp*(CO)Fe(P(OMe)2N(Ph)C(Me)N(H))]PF6 (896732-88-0)

Guidance literature:

With NaBH₄; In tetrahydrofuran; under N2 atm. to suspn. Fe complex in THF NaBH4 was added and stirred for 30 min at room temp.; soln. was evapd. to dryness, residue was dissolved in CH2Cl2 and chromed. on silica (CH2Cl2-acetone 9:1), soln. was dried in vacuo, residue was washed with ether and pentane and dried in vacuo; elem. anal.;

DOI:10.1021/om0510728

upstream raw materials:

P(N(SiMe₃)Ph)(OMe)2

Downstream raw materials:

[Cp*(CO)Fe(P(OMe)2N(Ph)C(Me)N(H))]PF₆

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