Technology Process of C13H16O3
There total 5 articles about C13H16O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 1h;
Inert atmosphere;
Reflux;
DOI:10.1002/anie.201301682
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium dihydrogenphosphate; zinc / acetone / 5 h / 20 °C / Inert atmosphere
2: ammonia / methanol / 20 °C / Inert atmosphere
3: pyridine / dichloromethane / 2.5 h / 0 °C / Inert atmosphere
4: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere; Reflux
With
pyridine; sodium dihydrogenphosphate; lithium aluminium tetrahydride; ammonia; zinc;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1002/anie.201301682
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 2.5 h / 0 °C / Inert atmosphere
2: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere; Reflux
With
pyridine; lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/anie.201301682