C₄₈H₃₃IO₄

Base Information

Chemical Name:C₄₈H₃₃IO₄
CAS No.:468751-21-5
Molecular Formula:C₄₈H₃₃IO₄
Molecular Weight:800.692
Hs Code.:

C<sub>48</sub>H<sub>33</sub>IO<sub>4</sub>

Synonyms:C₄₈H₃₃IO₄

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Chemical Property of C₄₈H₃₃IO₄

Chemical Property:

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Technology Process of C₄₈H₃₃IO₄

There total 10 articles about C₄₈H₃₃IO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 626-01-7
3-Iodoaniline

: 468751-21-5
C₄₈H₃₃IO₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: 6M HCl; NaNO₂

1.2: K₂CO₃ / acetonitrile; H₂O

2.1: pyrrolidine / Pd(Ph₃P)4; CuI

3.1: 85 percent / KOH; 18-crown-6 / tetrahydrofuran

4.1: nBuLi / tetrahydrofuran

5.1: I₂; MeI

6.1: 80.1 percent / Ph₃P / Pd(dba)2; CuI / triethylamine

7.1: 92.8 percent / I₂; MeI

8.1: Ph₃P / Pd(dba)2; CuI / triethylamine

9.1: I₂; MeI

10.1: 1M KOH / methanol; CHCl₃

With pyrrolidine; hydrogenchloride; potassium hydroxide; n-butyllithium; 18-crown-6 ether; iodine; triphenylphosphine; sodium nitrite; methyl iodide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; chloroform; triethylamine; 6.1: Sonogashira coupling / 8.1: Sonogashira coupling;
DOI:10.1016/S0040-4039(02)00539-7

Reference yield:

: 425436-17-5
3,3-diethyl-1-(3-iodophenyl)triaz-1-ene

: 468751-21-5
C₄₈H₃₃IO₄

Guidance literature:: Multi-step reaction with 9 steps

1: pyrrolidine / Pd(Ph₃P)4; CuI

2: 85 percent / KOH; 18-crown-6 / tetrahydrofuran

3: nBuLi / tetrahydrofuran

4: I₂; MeI

5: 80.1 percent / Ph₃P / Pd(dba)2; CuI / triethylamine

6: 92.8 percent / I₂; MeI

7: Ph₃P / Pd(dba)2; CuI / triethylamine

8: I₂; MeI

9: 1M KOH / methanol; CHCl₃

With pyrrolidine; potassium hydroxide; n-butyllithium; 18-crown-6 ether; iodine; triphenylphosphine; methyl iodide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; chloroform; triethylamine; 5: Sonogashira coupling / 7: Sonogashira coupling;
DOI:10.1016/S0040-4039(02)00539-7

Reference yield:

: 468751-09-9
C₁₃H₁₇N₃O

: 468751-21-5
C₄₈H₃₃IO₄

Guidance literature:: Multi-step reaction with 8 steps

1: 85 percent / KOH; 18-crown-6 / tetrahydrofuran

2: nBuLi / tetrahydrofuran

3: I₂; MeI

4: 80.1 percent / Ph₃P / Pd(dba)2; CuI / triethylamine

5: 92.8 percent / I₂; MeI

6: Ph₃P / Pd(dba)2; CuI / triethylamine

7: I₂; MeI

8: 1M KOH / methanol; CHCl₃

With potassium hydroxide; n-butyllithium; 18-crown-6 ether; iodine; triphenylphosphine; methyl iodide; copper(l) iodide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; methanol; chloroform; triethylamine; 4: Sonogashira coupling / 6: Sonogashira coupling;
DOI:10.1016/S0040-4039(02)00539-7