2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

Base Information

Chemical Name:2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol
CAS No.:1419875-41-4
Molecular Formula:C₁₉H₁₅Cl₂N₃O₂
Molecular Weight:388.253
Hs Code.:

Synonyms:2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

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Chemical Property of 2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

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Technology Process of 2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

There total 3 articles about 2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136815-80-0
1-[2-chloro-4-(4-chloro-phenoxy)-phenyl]-2-[1,2,4]triazol-1-yl-ethanone

: 16466-97-0,13254-27-8
1-propynylmagnesium bromide

: 1419875-41-4
2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

Guidance literature:: 1-[2-chloro-4-(4-chloro-phenoxy)-phenyl]-2-[1,2,4]triazol-1-yl-ethanone; With lanthanium (III) chloride bis(lithium chloride) complex; In tetrahydrofuran; at 20 ℃; for 1h;

1-propynylmagnesium bromide; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 119851-28-4
1-(2-chloro-4-(4-chlorophenoxy)phenyl)-ethan-1-one

: 1419875-41-4
2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: bromine

2.1: lanthanium (III) chloride bis(lithium chloride) complex / tetrahydrofuran / 1 h / 20 °C

2.2: 1 h / 20 °C

With lanthanium (III) chloride bis(lithium chloride) complex; bromine; In tetrahydrofuran;

Reference yield:

: 1419873-85-0
1-bromo-2-chloro-4-(4-chlorophenoxy)benzene

: 1419875-41-4
2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-([1,2,4]-triazol-1-yl)pent-3-yn-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride; isopropylmagnesium bromide; copper(l) chloride

2.1: bromine

3.1: lanthanium (III) chloride bis(lithium chloride) complex / tetrahydrofuran / 1 h / 20 °C

3.2: 1 h / 20 °C

With aluminum (III) chloride; lanthanium (III) chloride bis(lithium chloride) complex; bromine; isopropylmagnesium bromide; copper(l) chloride; In tetrahydrofuran;