2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

Base Information

Chemical Name:2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal
CAS No.:90406-06-7
Molecular Formula:C₂₈H₃₄F₃NO₇
Molecular Weight:553.576
Hs Code.:

Synonyms:2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

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Chemical Property of 2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

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Technology Process of 2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

There total 1 articles about 2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 667462-08-0
2-trifluoroacetamido-2-deoxy-α,β-D-glucopyranose

: 58886-34-3
2,2-dibenzyloxypropane

: 90406-06-7
2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

Guidance literature:: toluene-4-sulfonic acid; at 65 ℃; for 1.5h;
DOI:10.1016/0008-6215(84)85110-1

Reference yield: 98.0%

: 90406-06-7
2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

: 90406-10-3
2-deoxy-3,4-O-isopropylidene-2-(trifluoroacetamido)-D-glucose dibenzyl acetal

Guidance literature:: With water; In acetic acid; at 40 ℃; for 4h;
DOI:10.1016/0008-6215(84)85110-1

Reference yield:

: 90406-06-7
2-deoxy-3,4:5,6-di-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetal

: 90406-13-6
5,6-di-O-acetyl-2-deoxy-3,4-O-isopropylidene-2-(trifluoroacetamido)-aldehydo-D-glucose dibenzyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / water / aq. acetic acid / 4 h / 40 °C

2: pyridine

With water; In pyridine; acetic acid;
DOI:10.1016/0008-6215(84)85110-1